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Published January 15, 1970 | Published
Journal Article Open

Die Struktur von DL-μ-hydroxo-di-μ-nitro-bis(triamminkobalt)(3+)-trichlorid-hydrat

Thewalt, Ulf

Abstract

DL-μ-Hydroxo-di-μ-nitro-bis(triamminecobalt)(3 + )-trichloride hydrate, [(NH_3)_3Co(OH)(N0_2hCo(NH_3)_3]Cl_3. H_20, crystallizes in the monoclinic space group P2_1/c with ɑ = 9·70, b = 6-73, c = 24·57 Å and β = 104·3°; there are four formula units in the cell. The structure was determined by the heavy-atom method and refined by three-dimensional least-squares calculations. The final R index for 1397 observed reflections of non-zero weight is 0·067.

Additional Information

© 1970 International Union of Crystallography. Eingegangen am 5. Dezember 1968 und wiedereingereicht am 27. März 1969. This work was supported by Grant GP-5768 from the National Science Foundation.

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Created:
August 19, 2023
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