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Published June 1, 1973 | public
Journal Article

Nuclear Magnetic Resonance Spectroscopy. Application of Pulse and Fourier Transform Carbon-13 Nuclear Magnetic Resonance Techniques to Structure Elucidation. Rauwolfia Alkaloids

Abstract

The natural-abundance pulse and Fourier transform ^(13)C nmr spectra of several Rauwolfia alkaloids have been recorded. Using noise-decoupling, partial single-frequency off-resonance deooupling (SFOR), and lanthanide chelate induced chemical-shift changes (lanthanide shifts), a self-consistent series of assignments have been made for the observed resonances.

Additional Information

© 1973 American Chemical Society. Received October 24, 1972. Supported by the Public Health Service, Research Grant No. GM-11072 from the Division of General Medical Sciences, and by the National Science Foundation. National Institutes of Health Postdoctoral Fellow, 1971-1972. NATO Postdoctoral Fellow, 1970-1971.

Additional details

Created:
August 19, 2023
Modified:
October 24, 2023