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Published July 1, 1987 | public
Journal Article

Hydrogen depth profiling in solids: A comparison of several resonant nuclear reaction techniques

Abstract

Nuclear resonant reaction analysis (NRRA) techniques for hydrogen depth profiling in solid materials have typically used ion beams of 19F at the resonance energy of 16.44 MeV and 15N at 6.385 MeV. We report here the study of hydrogen analysis and profiles with the ^1H(^(19)F, ɑy)^(16)O reaction at the resonance energy of 6.42 MeV and investigation of the nuclear resonant reaction _1H(^(15)N ɑy)^(12)C at the resonance energy of 13.35 MeV as alternative means for hydrogen depth profiling. The results show that the method using the 6.42 MeV ^(19)F resonance has an excellent depth probe capability and moderate resolution as well as adequate sensitivity, and the method using the 13.35 MeV ^(15)N resonance provides a new tool with higher sensitivity and good depth resolution. The comparison of these four NRRA techniques under identical laboratory conditions is shown. Their characteristics and conditions of optimum utilization are discussed.

Additional Information

© 1987 Published by Elsevier B.V. Received 15 December 1986 and in revised form 11 February 1987. Available online 17 October 2002. Supported in part by the National Science Foundation [DMR83-18274]. We would like to thank Alan Rice, Engineer of the Caltech Tandem Laboratory, for his assistance with ^(15)N ion beam generation, and D. Weathers and Dr. X.A. Zhao for their help with the proton implantation. We also acknowledge our gratitude to Professor G.R. Rossman, Division of Geological Sciences, Caltech, for providing tourmaline standards and to Professor J.E. Ericson, University of California at Irvine, for the hydration of tektite samples. On of the authors (F.R.) acknowledges the financial support by the Deutsche Forschungsgemeinschaft.

Additional details

Created:
August 19, 2023
Modified:
October 18, 2023