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Published November 1990 | Supplemental Material
Journal Article Open

Octakis(2,6-diethylphenyl)octastannacubane

Abstract

Thermolysis of hexakis(2,6diethylphenyl)-cyclotristannane (2) in naphthalene provides red octakis-(2,Gdiethylphenyl)octastannacubane (l), which has been fully characterized, including crystallographic analysis. Compound 1 represents the first example of the organostannane cluster series (RSn)_n.

Additional Information

© 1990 American Chemical Society. Received July 24, 1990. We thank Dr. Cynthia Day of Crystalytics Co. for the structural analysis of 1 and the National Science Foundation (Grant CHE-9001462) for support of this work. High-resolution mass spectra were provided by Dr. Catherine Costello of the facility supported by the National Institutes of Health (Grant R-R-00317; principal investigator Professor K. Biemann), from the Division of Research Resources.

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August 19, 2023
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