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Published January 1996 | Published + Supplemental Material
Journal Article Open

A Pinacol Precursor to a Chiral Spiro Compound

Abstract

The dimer of 1-indanolyl obtained from the UV photolysis of 1-indanone in 2-propanol is trans-α,α'-biindanyl-α,α'-diol, (C_9H_9O)_2. There are two almost identical molecules in the asymmetric unit linked by a hydrogen-bonding system that extends along the a axis. Bond distances and angles are as expected.

Additional Information

© 1996 International Union of Crystallography. (Received 11 January 1995: accepted 27 July 1995) Data collection: CAD-4 Software (Enraf-Nonius, 1989). Cell refinement: CAD-4 Software. Data reduction: CRYM (Duchamp, 1964). Program(s) used to solve structure: CRYM. Program(s) used to refine structure: CRYM. Molecular graphics: ORTEPII (Johnson, 1976). Software used to prepare material for publication: CRYM.

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Supplemental Material - sendcif_sz1046sup1

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Created:
August 20, 2023
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October 18, 2023