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Published May 18, 2016 | Supplemental Material
Journal Article Open

High Field Solid-State NMR Spectroscopy Investigation of ^(15)N-Labeled Rosette Nanotubes: Hydrogen Bond Network and Channel-Bound Water

Abstract

^(15)N-labeled rosette nanotubes were synthesized and investigated using high-field solid-state NMR spectroscopy, X-ray diffraction, atomic force microscopy, and electron microscopy. The results established the H-bond network involved in the self-assembly of the nanostructure as well as bound water molecules in the nanotube's channel.

Additional Information

© 2016 American Chemical Society. Received: March 6, 2016. Publication Date (Web): May 04, 2016. Access to the 900 MHz NMR spectrometer was provided by the National Ultrahigh Field NMR Facility for Solids, a national research facility funded by the Canada Foundation for Innovation, the Natural Sciences and Engineering Research Council of Canada (NSERC), the Ontario Innovation Trust, Recherche Québec, the National Research Council Canada (NRC), and Bruker BioSpin and managed by the University of Ottawa. We thank NSERC, NRC, the University of Alberta, and Northeastern University for financial support. The authors declare no competing financial interest.

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Created:
August 20, 2023
Modified:
October 18, 2023